Synthesis and characterization of dimethacrylate macromonomer using maghnite-h+as an eco-friendly catalyst
نویسندگان
چکیده
The dimethacrylate macromonomer named bis (2-hydroxy-3-(méthacryloyloxy) propyl) fumarate (HMPF) was synthesized by ring opening reaction of epoxide function glycidyl methacrylate (GMA) with maleic anhydride (MA) in presence Maghnite-H+ as a catalyst at room temperature and free solvent. is proton exchanged montmorillonite clay it an Algerian activated sulfuric acid 0,23M. HMPF characterized FT-IR, 1H NMR 13C spectroscopic techniques. A kinetic study carried out to determine the amount (5, 10, 20 30%) which will give abetter yield synthesis reaction. T he 62. 2 3% for quantity (20% relative monomer r eaction time 72 h.
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ژورنال
عنوان ژورنال: Journal of Fundamental and Applied Sciences
سال: 2023
ISSN: ['1112-9867']
DOI: https://doi.org/10.4314/jfas.v12i2.19